GB/T 23207-2008 河豚鱼、鳗鱼和对虾中485种农药及相关化学品残留量的测定 气相色谱-质谱法

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基本信息
标准名称:河豚鱼、鳗鱼和对虾中485种农药及相关化学品残留量的测定 气相色谱-质谱法
英文名称:Determination of 485 pesticides and related chemicals residues in fugu,eel and prawn—GC-MS method
中标分类: 食品 >> 食品综合 >> 基础标准与通用方法
ICS分类: 食品技术 >> 食品试验和分析的一般方法
发布部门:中华人民共和国国家质量监督检验检疫总局 中国国家标准化管理委员会
发布日期:2008-12-31
实施日期:2009-05-01
首发日期:2008-12-31
作废日期:
主管部门: 国家标准化管理委员会
提出单位:中华人民共和国国家质量监督检验检疫总局
归口单位:中华人民共和国国家质量监督检验检疫总局
起草单位:中华人民共和国秦皇岛出入境检验检疫局、山东农业大学
起草人:庞国芳、郑锋、范春林、王明林、刘永明、曹静
出版社:中国标准出版社
出版日期:2009-05-01
页数:【胶订-大印张】76页
计划单号:20079490-T-469
适用范围

本标准规定了河豚鱼、鳗鱼和对虾中485种农药及相关化学品(参见附录A和附录F)残留量气相色谱-质谱测定方法。
本标准适用于河豚鱼、鳗鱼和对虾中485 种农药及相关化学品残留的定性鉴别,也适用于对其中402种农药及相关化学品进行定量测定。

前言

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目录

前言Ⅲ 1 范围1 2 规范性引用文件1 3 原理1 4 试剂和材料1 5 仪器2 6 试样制备与保存2 7 测定步骤2 8 结果计算4 9 精密度4 附录A (资料性附录) 485种农药及相关化学品中文与英文名称、方法检出限、分组、溶剂选择和 混合标准溶液浓度5 附录B (资料性附录) 485种农药及相关化学品和内标化合物的保留时间、定量离子、定性离子及定量离子与定性离子的丰度比值20 附录C (资料性附录) A、B、C、D、E、F六组农药及相关化学品选择离子监测分组表35 附录D (资料性附录) 标准物质在河豚鱼基质中选择离子监测GCMS图41 附录E (资料性附录) 485种农药及相关化学品精密度数据表47 附录F (资料性附录) 485种农药及相关化学品英文中文名称对照索引(按英文字母顺序) 62

引用标准

下列文件中的条款通过本标准的引用而成为本标准的条款。凡是注日期的引用文件,其随后所有的修改单(不包括勘误的内容)或修订版均不适用于本标准,然而,鼓励根据本标准达成协议的各方研究是否可使用这些文件的最新版本。凡是不注日期的引用文件,其最新版本适用于本标准。
GB/T6379.1 测量方法与结果的准确度(正确度与精密度) 第1部分:总则与定义
(GB/T6379.1—2004,ISO5725-1:1994,IDT)
GB/T6379.2 测量方法与结果的准确度(正确度与精密度) 第2部分:确定标准测量方法重复
性与再现性的基本方法(GB/T6379.2—2004,ISO5725-2:1994,IDT)
GB/T9695.19 肉与肉制品 取样方法(GB/T9695.19—1988,neqISO/DIS3100-1:1984)

所属分类: 食品 食品综合 基础标准与通用方法 食品技术 食品试验和分析的一般方法
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【英文标准名称】:Crossrecessedcountersunk(flat)headtappingscrews(commonheadstyle);identicalwithISO7050:1983
【原文标准名称】:十字槽沉头(扁平头)自攻螺钉(普通头型)
【标准号】:DINISO7050-1990
【标准状态】:作废
【国别】:德国
【发布日期】:1990-08
【实施或试行日期】:
【发布单位】:德国标准化学会(DE-DIN)
【起草单位】:FMV
【标准类型】:()
【标准水平】:()
【中文主题词】:自攻丝螺钉;尺寸;螺钉;十字头紧固件;螺纹;埋头紧固件;凹槽头螺钉;紧固件;沉头螺钉;名称与符号;材料
【英文主题词】:Acceptancespecification;Commonheads;Countersunkfasteners;Countersunkheadscrews;Countersunk-headtappingscrew;Crossrecessedscrews;Cruciform-headfasteners;Deliveryconditions;Designations;Dimensions;Fasteners;Materials;Recesses;Screws(bolts);Self-tappingscrews;Specification(approval);Threads;Tolerances(measurement)
【摘要】:Thisstandardcontainsdimensionalandtechnicalrequirementsofcrossrecessedcountersunk(flat)headtappingscrews(commonheadstyle)andspecifiestheirdesignation.
【中国标准分类号】:J13
【国际标准分类号】:21_060_10
【页数】:6P.;A4
【正文语种】:德语


MIL-STD-1678/2, DEPARTMENT OF DEFENSE STANDARD PRACTICE: FIBER OPTIC CABLING SYSTEMS REQUIREMENTS AND MEASUREMENTS(PART 2: OPTICAL MEASUREMENTS) (PART 2 OF 5 PARTS) (28 MAY 2010) [SUPERSEDING DOD-STD-1678]., This standard practice provides detailed information and guidance to personnel concerned with ensuring standardization of fiber optic cable topologies (optical fiber cabling and associated components) on military mobile vehicles used in air, land, and sea applications. In general, the requirements and methods specified herein are not identifiable to any specific mobile vehicle class or type, but are intended to standardize and minimize variations in requirements, test setups, test measurement procedures, test sample fabrication configurations, and other aspects that must be addressed for completeness. Where specified, constrains for usage or platform types will be listed. The term 損latform?will be used to refer to the military mobile vehicles in general or, where designated, one particular class (such as 揳ircraft platform? or one particular type within that class (such as 揊-35?.4. In order to provide flexibility in the use and update of the different aspects for requirements and methods, this standard practice is issued in five parts; as follows:Part 1: Design, installation and maintenance requirements. This part addresses design requirements for platforms that use cable harnesses as the means to transport data through optical fiber among communication network and end user equipment. Larger platforms that route trunk cables through cableways and drop cables to the end user (application equipment), can cite applicable requirements in Part 1 of the Standard Practice and augment them with use of MIL-HDBK-2051 and MIL-STD-2042 as appropriate. Surface ships and submarines, are to use MIL-HDBK-2051 and MIL-STD-2042 in lieu of Part 1 of this Standard Practice.Part 2 Optical measurements. Part 2 of this standard practice addresses further details to refine or bound (constrain) the performance of each optical test measurement addressed. The test methods, such as those in a TIA-455 series standard or military standard/specification, are cited already. This part of the standard practice augments the test method in the standard or specification to ensure consistency with setup and measurement procedure. This consistency minimizes variations when comparing data obtained from different test laboratories (including commercial, vendor, Government and Government contractor).Part 3 Physical, mechanical, environmental and material measurements. Part 3 of this standard addresses further details to refine or bound (constrain) the performance of each physical, mechanical, environmental and material test measurement or inspection addressed. The test methods, such as those in a TIA-455 series standard or military standard/specification, are cited already. This part of the standard practice augments the test method to ensure consistency with setup, measurement procedure, data recording/analysis and other factors critical to conducting or evaluating test performance. This consistency minimizes variations when comparing data obtained from different test laboratories (including commercial, vendor, Government and Government contractor).Part 4 Test sample preparation/fabrication requirements. Part 4 of this standard practice addresses further details to refine or bound (constrain) the preparation and fabrication of test samples for the fiber optic components addressed. Fabrication methods, such as those in the Shipboard installation standard, MIL-STD-2042, or in the general series aircraft maintainer抯 manual, NAVAIR 01-1A-505-4/TO 1-1A-14-1, are cited already. This part of the standard practice augments the fabrication method to ensure consistency of the test configurationPart 5 Design phase and legacy measurements. Tests that are more unique to the design phase are addressed in Part 5 of this standard practice. Also, Part 5 addresses some test methods cited in former DOD-STD-1678. The test methods cited in DOD-STD-1678 are considered obsolete; however, a few military specifications and commercial standards still refer to some of the test methods. These test methods are provided in this part of the standard practice with the recommended replacement method. These latter test methods are listed under the constraint that they be used only with the specific military specifications or commercial standards in which they are cited. The intent is to delete each DOD-STD-1678 test method from that standard practice in Part 5 once its reference from military specification or commercial standard is removed.